Formation And Stabilization Of ZnO Nanoparticles Inside MCM-48 Porous Support Via Post-synthetic Organometallic Route
Mahuya Bandyopadhyay1*, Hermann Gies2, Wolfgang Grünert3, Maurits Van Den Berg4, Alexander Birkner5
1Institute of Infrastructure, Technology, Research and Management, IITRAM, Maninagar, Ahmedabad, Gujarat, India
2Laboratory of Crystallography, Ruhr University Bochum, 44780 Bochum, Germany
3Laboratory of Industrial Chemistry, Ruhr University Bochum, 44780 Bochum, Germany
4Sachtleben Pigment GmbH, 47829, Krefeld, Germany
5Laboratory of Physical Chemistry I, Ruhr University Bochum, 44780 Bochum, Germany
Adv. Mater. Lett., 2015, 6 (11), pp 978-983
DOI: 10.5185/amlett.2015.5963
Publication Date (Web): Oct 26, 2015
Copyright © 2019 VBRI Press
E-mail: mahuyabandyopadhyay@iitram.ac.in
The interpenetrating 3-dimensional channel system of silica MCM-48 has been selected for the deposition of ZnO nanoparticles. The post-synthetic organometallic route was employed to load the mesoporous silica with ZnO-precursor molecule. Calcination of the composite transformed the organometallic sorbate to the corresponding metal oxide. X-ray powder diffraction, N2-Adsorption and TEM measurement have supported the efficient loading and growth of ZnO particles in the channels of mesoporous silica matrix. EXAFS analysis (ZnK-edges) also complemented the metal uptake. Presence of nano-dispersed and nanosized ZnO particles confined by the mesoporous pore system was established by TEM and EXAFS analysis.
Healthcare informatics driven nanotechnology
Brief Review: Simulation of Novel Systems Using Duality Quantum Algorithm
Significant Quality Parameters of Finishing Technology in Offset Printing on Solid Board Boxes Depending on the type of Material
Generation of entanglement in spin states of Rydberg atoms by chirped optical pulses
Matrix and Variant Transformations Simulate Statistical Canonical Ensembles from Fock to Poissonian States of Random Sequences
The Vortex Glass-Liquid Transition in Fe1.02Se Crystal
Magnetic Properties of Intercalated Gr/Ni (111) System
Functionalized Nano Carbon for excellent Microwave Absorption at GHz Frequency
Deformation Texture Modelling by Mean-Field and Full-Field Approaches
Growth, Linear and Nonlinear Optical Studies of D-Tartaric Acid Crystal
Graphene-MoS2-Au-TiO2-SiO2 Hybrid SPR Biosensor for Formalin Detection: Numerical Analysis and Development
Microstructure and Mechanical Characterization Study in the IN718/BNi-2/316L Joint by Transient Liquid Phase Bonding Process
Stress Fields at the Central Point of Arc Crack under Uniaxial Tension
Cloud Medicine set to Revolutionize Doorstep Personalized Healthcare
Various surfactants for 0 – 3 dimensional nanocarbons: Separation, exfoliation and solubilization
Polypyrrole based biofunctional composite layer for bioelectrocatalytic device system
Innovative Graphene-PDMS sensors for aerospace applications
Effect of hot drawing process and carbonization temperature in electrochemical behavior of electrospun carbon nanofibers
Chemical Reactivity and Electronical Properties of Graphene and Reduced Graphene Oxide on Different Substrates
Laser Raman micro-spectroscopy as an effective non-destructive method of detection and identification of various sp2 carbon modifications in industry and in nature
Electrochemical promotion of ammonia synthesis with proton-conducting solid oxide fuel cells
Biomimetic surfaces with hierarchical structure using microsized texture and nanosized Cu particles for superhydrophobicity
Enhancement the properties of high and low-density polyethylene membranes by radiation grafting process
Synthesis of 9-Aminoacridine and its Application as an Anode Material for Aqueous Rechargeable Lithium–ion Batteries
Facile synthesis of novel tough and highly flexible biodegradable membranes for water microfiltration
Investigating the possibility of using acetic acid in place of HF in chromium-benzenedicarboxylates (MIL-53 and MIL-101) synthesis applicable for CO2 adsorption
Copyright ©2010-2019 VBRI Press
Full Article