1Department of Physics, Chittagong University of Engineering and Technology, Chittagong, Bangladesh
2Department of Physics, Bangladesh University of Engineering and Technology, Dhaka, Bangladesh
Adv. Mater. Lett., 2015, 6 (9), pp 810-815
DOI: 10.5185/amlett.2015.5854
Publication Date (Web): Sep 06, 2015
Copyright © IAAM-VBRI Press
E-mail:belalcuet@gmail.com
The influence of Al3+ substitution on the microstructure and impedance spectroscopy of Ni0.27Cu0.10Zn0.63AlxFe2-xO4 has been studied by scanning electron microscopy and impedance analyzer where the formation of the material in the spinel crystal structure was initially confirmed by X-ray structural analysis with room temperature data. The surface morphology indicates well defined grains separated by grain boundaries and with Al substitution average grain size decrease from 17 μm to 12 μm and zinc losses as well. The complex-plane impedance spectra indicate that the material can be represented by two semicircular arcs (its tendency) which corresponds to the bulk and the grain boundary resistance at high and low frequencies respectively. With Al substitution both grain and grain boundary resistance increases from 7.48 kΩ to 15.62 kΩ and 92.34 kΩ to 192.46 k respectively. Electric modulus spectra reflect the contributions from grain and grain boundary effects: the large resolved semicircle arc caused by the grain effect and the small poorly resolved semicircle arc was attributed to the grain boundary.
Surface morphology, impedance spectroscopy, enhanced grain and grain boundary resistance, resolve relaxation.
Water and Sanitation Management: During and after COVID-19 Pandemic
Polymeric Energy Materials: Development and Challenges
Influence of Different Copolymer Based Compatibilizers on Performance of Pristine and Recycled PP/PE blends
Bio Ceramics: New Material from Mangrove Bark
Hybrid Physical Chemical Vapour Deposition (HPCVD) of Superconducting MgB2 Thin Films on three Dimensional Copper Substrates
Photoinduced Electron Transfer Reactions of tris(4,4’-dimethoxy-2,2’-bipyridyl)ruthenium(II)cation with Quinones in Aqueous Medium
A Comparative Study of Green Synthesized AgNPs using Carissa Carandas and Nerium indicum Leaves and its Activities against Selected Human Pathogens and MCF 7 Cell
Design and Modelling of Carbon Fiber Grid Structure based Carbon/Epoxy Composites for Enhanced Microwave Absorbing Properties
Elaboration and Characterization of Macroporous Bioceramics using Polymeric Sponge Replication Method
Advanced Healthcare Biomaterials
Piezoelectric Alternative Energy Sources as a Part of the Global Energy Concerns – Future Prospects in the Science and Market
Rectify the Injury-Induced Microenvironment Imbalance in Peripheral Nerve Repair
A Mini Review on Biodegradable Magnesium Alloy Vascular Stent
Prospective Applications of Marine Oriented Materials in the Repair of Peripheral Nerve Injury
Design and Implementation of Dynamic FPAA Based Interface Circuit for Thin Film Lead-Free Piezoelectric Sensors
An Аpproach for Nanostructuring of Piezoelectric Materials by Template-assisted Growth in Porous Aluminum Oxide
Study of Sputtered Barium Strontium Titanate Films for Energy Harvesting Applications
The Effect of Bias on Properties of DLC Coatings for Artificial Joints
Fabrication of Tens-micron-sized Functionalized Polystyrene Microspheres for Utilization in Chiral Drug Isolation
Copyright ©2010-2020 VBRI Press
Full Article